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To decrease wear and friction, zinc dialkyldithiophosphate (ZDDP) has been used in engine oil for several decades, but the mechanism of the tribofilm formation is still unclear. The purpose of this study is to characterize the chemical details of the tribofilm by using high-resolution approaching.

An ISO VG 100 mineral oil mixed with ZDDP was used in sliding tests on cylindrical roller bearings. Tribofilm formation was observed after 2 h of the sliding test. X-ray photoelectron spectroscopy (XPS) and atom probe tomography (APT) were used for chemical analysis of the tribofilm.

The results show that the ZDDP tribofilm consists of the common ZDDP elements along with iron oxides. A considerable amount of zinc and a small amount of sulfur were observed. In particular, an oxide interlayer with sulfur enrichment was revealed by APT between the tribofilm and the steel substrate. The depth profile of the chemical composition was obtained, and a tribofilm of approximately 40 nm thickness was identified by XPS.

A sulfur enrichment at the interface is observed by APT, which is beneath an oxygen enrichment. The clear evidence of the S interlayer confirms the hard and soft acids and bases principle.

The peer review history for this article is available at: https://publons.com/publon/10.1108/ILT-01-2020-0035/

The purpose of this paper is to study the influence of dimple textures on the friction and wear properties of tapered roller bearings (TRBs) with many pattern parameters, e.g. diameter, depth and area density under starved lubrication.

The pattern parameters include the dimple diameter (D; 60, 100 and 200 µm), dimple depth (H; 5, 10 and 20 µm) and area density (S; 6%, 12% and 24%). Dimples were fabricated on the outer ring (OR) of TRBs using a laser marking machine. The tribological properties of dimple-textured TRBs under starved lubrication were studied on a vertical universal friction wear tester with special friction pairs. The effect mechanisms of dimple textures on the tribological properties of TRBs are presented and summarized through experiments and discussions.

When dimple-textured TRBs revolve under starved lubrication, the average coefficients of friction (ACOF) and wear losses are markedly lower than those of non-textured bearings. S has the greatest influence on the COF curve. When D is 100 µm and S is 24%, the ACOF and wear losses are both lowest, i.e. 0.00426 and 0.51 mg, respectively. Under the same test conditions, compared with the non-textured group, its COF and wear loss decreased by 35.6% and 62.5%, respectively.

This work provides a useful reference for the research on the raceways of textured TRBs.